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氟代碳酸乙烯酯的測定毛細(xì)管柱
氟代碳酸乙烯酯的測定毛細(xì)管柱 詳細(xì)信息：

名稱：鍵合型毛細(xì)管柱

固定相：50%苯基-50%二甲基聚硅氧烷

規(guī)格：30m*0.53mm*1.0um
型號：OV-17
應(yīng)用：HGT 4-2014 氟代碳酸乙烯酯

以碳酸乙烯酯為原料，經(jīng)氯化反應(yīng)生成中間體一氯碳酸乙烯酯；一氯碳酸乙烯酯與三乙胺脫氯化氫后得到目標(biāo)產(chǎn)物碳酸亞乙烯酯；一氯碳酸乙烯酯與氟化鉀發(fā)生取代反應(yīng)后得到目標(biāo)產(chǎn)物氟代碳酸乙烯酯。

浩瀚色譜（山東）應(yīng)用技術(shù)開發(fā)有限公司采用氣相色譜對目標(biāo)產(chǎn)物和中間體進(jìn)行了結(jié)構(gòu)表征和定量分析，研究結(jié)果均證實了化合物的化學(xué)結(jié)構(gòu)。研究還通過單因素實驗，對各步工藝條件進(jìn)行了優(yōu)化，證實了工藝路線的可行性。

氟代碳酸乙烯酯的測定毛細(xì)管柱  測試譜圖：




Capillary column for the determination of fluoroethylene carbonate
Capillary column for the determination of fluoroethylene carbonate Details:

Name: Bonded Capillary Column

Stationary phase: 50% phenyl-50% dimethylpolysiloxane

Specifications: 30m*0.53mm*1.0um
Model: OV-17
Application: HGT 4-2014 Fluoroethylene carbonate



Using ethylene carbonate as a raw material, the intermediate ethylene monochlorocarbonate is generated by chlorination reaction; the target product vinylene carbonate is obtained after dehydrochlorination of ethylene monochlorocarbonate and triethylamine; ethylene monochlorocarbonate and potassium fluoride are generated After the substitution reaction, the target product fluoroethylene carbonate is obtained.

Haohan Chromatography (Shandong) Application Technology Development Co., Ltd. used gas chromatography to characterize and quantitatively analyze the target products and intermediates. The research results confirmed the chemical structures of the compounds. The research also optimized the process conditions of each step through single factor experiments, which confirmed the feasibility of the process route.

Determination of fluoroethylene carbonate capillary column Test spectrum: